Show simple item record

dc.contributor.authorWellkamp, Marvin
dc.contributor.authorGarcía Camacho, Francisco
dc.contributor.authorDurán Riveroll, Lorena M.
dc.contributor.authorTebben, Jan
dc.contributor.authorTillmann, Urban
dc.contributor.authorKrock, Bernd
dc.date.accessioned2020-10-20T11:14:11Z
dc.date.available2020-10-20T11:14:11Z
dc.date.issued2020-09-29
dc.identifier.issn1660-3397
dc.identifier.urihttp://hdl.handle.net/10835/8693
dc.description.abstractAmphidinols are polyketides produced by dinoflagellates suspected of causing fish kills. Here, we demonstrate a liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the identification and quantification of amphidinols (AM). Novel AM were detected by neutral loss (NL) scan and then quantified together with known AM by selection reaction monitoring (SRM). With the new method, AM were detected in four of eight analyzed strains with a maximum of 3680 fg toxin content per cell. In total, sixteen novel AM were detected by NL scan and characterized via their fragmentation patterns. Of these, two substances are glycosylated forms. This is the first detection of glycosylated AM.es_ES
dc.language.isoenes_ES
dc.publisherMDPIes_ES
dc.rightsAttribution-NonCommercial-NoDerivatives 4.0 Internacional*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/*
dc.subjectphycotoxines_ES
dc.subjectichthyotoxines_ES
dc.subjectdinoflagellatees_ES
dc.subjectharmful algaees_ES
dc.subjectglycosylationes_ES
dc.titleLC-MS/MS Method Development for the Discovery and Identification of Amphidinols Produced by Amphidiniumes_ES
dc.typeinfo:eu-repo/semantics/articlees_ES
dc.relation.publisherversionhttps://www.mdpi.com/1660-3397/18/10/497es_ES
dc.rights.accessRightsinfo:eu-repo/semantics/openAccesses_ES


Files in this item

This item appears in the following Collection(s)

Show simple item record

Attribution-NonCommercial-NoDerivatives 4.0 Internacional
Except where otherwise noted, this item's license is described as Attribution-NonCommercial-NoDerivatives 4.0 Internacional